Retro Reflection PROBE For In-Line Color Measurement

MONITORING CHEMICAL REACTIONS

During a chemical reaction, reactants are consumed, products and byproducts are formed, and contaminants may be introduced.

Using in-line fiber optic spectrophotometers, chemical producers can measure the UV-Vis light absorbance (Fig. 1) and the concentration (depletion
or production) of reactants, products, byproducts, and contaminants in real-time.

Chemical reactions occur at different speeds, and therefore, real-time information about the reaction’s stoichiometry (i.e. proportionality) between reactants and products is critical.

Combining in-line UV-Vis fiber optic spectroscopy with process control instrumentation enables production systems to respond immediately to
process changes, guaranteeing total quality control, minimizing waste and preventing unexpected downtime.

Equitech’s Retro-Reflection Probe (RRP) (Fig. 2) is a rugged, high throughput probe developed for use in industrial process environments. The probe can operate at temperature from -30°C to 280°C and at pressures up to 206 bar (3000 psi).

Chemical concentration
FIG 1. CHEMICAL CONCENTRATION CHANGES

UV-VIS SPECTROSCOPY

UV-Vis spectroscopy is a quantitative technique that measures the amount of ultraviolet (UV) and visible light that is absorbed by a substance.

It also used to measure the concentration of reactants, products and impurities in chemical reactions, mixing and blending unit operations.

This determination is possible due to a relationship of proportionality between the substance’s absorbance and its concentration, known as the Beer Lambert’s
Law expressed as:

A = εLc

where:
A = Amount of light that the sample absorbs at a specific wavelength
ε = Molar absorbing coefficient or absorptivity of the absorbing species
L = Optical path length
C = Concentration of the absorbing species
 

Retro Reflection Probe
FIG 2. RETRO REFLECTION PROBE
OpticalSpecifications
Flow Channel Gap (GFC) 2, 5, 10, 20, or 50 mm
Lens/Window MaterialUV or NIR fused silica*
Numerical Aperture 0.32 NA
Reflector MaterialBack surface Al / silica*
EfficiencyTypical: 30% at 500nm**
Optical Fiber TypeUV or NIR 400/440 silica on silica†
Fiber PackagingPVC-coated (80°C) armored duplex Teflon coated (280°C)
armored duplex
Fiber Length5 meters standard
Fiber TerminationSMA 905
* Other materials available upon request
** Efficiency measured relative to direct fiber connection between light source and detector using 400 micron core fiber optic
† Other lengths available upon request
PhysicalSpecifications
Body & Extension Materials316 SS**
Body Dimensions (LB)[ 38.1 mm (1.5”) + GFC ] x 12.7mm (0.5”) OD
Extension Tube Dimensions (LET)Standard Length 203.2mm (8”) L x 12.7mm (0.5”) OD†
Seal TypeO-ring
Seal MaterialKalrez® 6375
Temperature Range-30°C to 280°C
Maximum Pressure207 bar (3000 psi)
** Efficiency measured relative to direct fiber connection between light source and detector using 400 micron core fiber optic
† Other lengths available upon request
Kalrez® is a registered trademark of DuPont Dow® Elastomers
Teflon® is a registered trademark of DuPont
Retro Reflection Probe

CONTACT US

Equitech Int’l Corporation
7711 Idlewild Road, Indian Trail, NC 28079
Tel +1-704-882-4624
[email protected]
equitechintl.com